SEDIMENT PROPERTIES 5.22
glass fiber filter in a Gooch crucible. The filter containing the sediments is then oven-
dried, cooled in a desiccator, and weighed. Sediment weight is computed as the final less
the original (tare) weight. Filtration has the advantage of eliminating the need to
compensate for dissolved solids in the water, and it can also be more rapid that the evap-
oration method. However, filter media will quickly become clogged if more than several
hundred milligrams per liter of fines is present.
5.6.2 Evaporation Method
In the evaporation method, the sample is first allowed to settle to the bottom of the
sample bottle. Settling time depends on the nature of the sediment; for clays, settling may
require weeks and small amounts of flocculant may have to be added. Samples should
settle in the dark to prevent biological growth. After settling, the supernatant is discarded
and the residual aliquot of native water (usually about 20 to 50 mL) is poured into an
evaporating dish, and distilled water is used to rinse the remaining sediment. After the
water is evaporated without boiling, the dry sample is heated to 110°C for at least 1 h,
then cooled in a desiccator and weighed. A correction for dissolved solids should be
made in waters high in dissolved solids or low in suspended solids. The weight of
dissolved solids is determined by evaporating a sample aliquot of settled or filtered water.
If dissolved solids constitute a significant percentage of the total solids in the sample, a
correction should be made. In environments having relatively stable dissolved solids
levels, using a constant-volume aliquot of native water in all samples that are evaporated
produces a constant correction factor.
5.6.3 Specific Gravity Bottle
With the specific gravity of water known as a function of temperature, the sediment con-
tent in a sample can be measured as the difference between the weight of clear native
water (not distilled water), and of the sample when weighed in a specific gravity bottle.
This method has the advantage of providing almost instantaneous values of sediment
concentration because it does not require sample desiccation. It is therefore well-suited
for field monitoring during operations such as reservoir flushing. It can be used with any
size of sediment. The tare weight of each bottle should be recorded when it is filled with
clear native water, all bubbles must be carefully eliminated from within the stoppered
bottle, and the bottle exterior must be carefully dried before weighing. For field use, the
balance must be placed in an area completely unaffected by vibration, such as may occur
in machinery buildings. Because this method measures the small differences in weighs
between 100 mL of clear water and the same volume of turbid water, contained in a
bottle weighing about 40 g, it is best used for sediment concentrations exceeding 250
mg/L
5.6.4 Sediment Volume
In streams where most or all sediments are sands, the sediment can be settled in an
Imhoff cone, and the sediment content expressed as milliliters per liter. This method is
useful in monitoring sediment release events because results can be obtained after short
settling time, on the order of 1 min. However, this method requires that a calibration
curve be constructed for each site where this method is used, to develop a relationship
between settled sediment volume and sediment mass. During every event when this
method is used, several samples should be collected and analyzed in a laboratory to
confirm the original calibration. Because the grain size distribution can change
significantly over the course of an event, it is also important that samples be taken at
different periods as the calibration curve may shift during an event. In addition to speed,
this method has the advantage of simplicity in equipment and procedure.