950
Chapter
I4
5.
Halogen diode detector probe test
6.
Helium mass spectrometer detector (sniffer) probe technique
7.
Helium mass spectrometer tracer probe technique
8.
Helium mass spectrometer hood method.
Tests for gross leaks involve direct visual inspection for signs of tracers or leakage prod-
ucts, or scanning of leaking systems with an ultrasonic leak detector to locate the sources of
hissing sounds. Small leaks can be detected by sophisticated leak testing methods utilizing
tracer gases such as halogen vapors and helium with detectors such as the heated anode halogen
detector and the helium mass spectrometer, respectively. Leak testing methods listed in items
1
to 8 are discussed next. Yet another method of leak testing is acoustic emission testing, and
this method is explained in the section on acoustic emission.
Ultrasonic Leak Detection
The leakage of a gas through small openings, even for small pressure differences, generates
noise in the ultrasonic range. Therefore, it
is
possible to detect the leaks by listening for them
using an ultrasonic listening device, which can record low noise levels produced
in
the high
frequencies (40-50 kHz) that occur due to turbulent flow [34].
Bubble Testing
Bubble testing can be performed by the direct pressure technique or vacuum-box technique.
The direct pressure technique using bubble solution is the more common one.
Bubble Testing, Direct Pressure Technique.
The objective of the direct pressure technique is
to locate leaks in a pressurized component by application of a solution or by immersion
in
liquid that will form bubbles as the leakage gas passes through it. To perform this test, pressur-
ize the shell with inert gas or air; the required pressure differential can be from 1 kgkm’ to
1.25 times the design pressure of the vessel but less than
20
kg/cm’. After sufficient pressure
soak
time, apply a soap solution over the joints. Generally the surfaces must be in the tempera-
ture range of 40-125°F (4.5-52°C). This method can detect leaks of the order of
10-s
pascal
m’/sec when the test objects are immersed in detection liquids.
Bubble Testing, Vacuum Box Technique.
The objective of the vacuum box technique is to
locate leaks in a pressure boundary that cannot be directly pressurized. In this method, on one
side of the test joint after application of soap solution, vacuum is created and
if
there are any
through leaks, atmospheric air from the other side will come out to the vacuum side and will
be observed as the formation of a bubble.
Gas Leak Lake Testing
For this method, pressurize the shell side of the heat exchanger with air or nitrogen to the
maximum allowable working pressure
(MAWP)
at room temperature, set the unit vertically.
With a ring of about 2
in
height (50.8 mm), make a dam on the tubesheet face. Fill the tube
side with water to the level of the dam, and observe for bubbles.
Pressure Change Test
This test method describes the technique for detecting the leakage rate of the boundaries of a
closed compartment or the vessel at a specific pressure or vacuum by indicating pressure or
vacuum change over the given time period.
Halogen Diode Detector Testing
Principle.
A
detector or a sniffer sucks a mixture of air and leaking tracer gas through a
tubular probe into an instrument that is sensitive to small amounts of tracer gas. The tracer
gas
can be a halide gas (Refrigerant 12) to a maximum of 25% of the design pressure.
A
heated