5th ed. An Imprint of Elsevier Science, 2003. – 634 p. -
The only complete source that covers the purification of laboratory chemicals that are commertially available in such an easy-to-use format
- Provides purification procedures for commercially available chemicals and biochemicals
- Includes an extremely useful compilation of ionisation constants
Now in its fifth edition, Purification of Laboratory Chemicals continues to ratory scientists with a manual for purifying and increasing the purity of, mode commercially available chemical substances.
The authors have written and revised six chapters that describe the aspects of purification and properties of chemical substances. In addition to detailing physical methods and procedures such as crystallization, distillation, chromatography, etc. , the authors also address cheinical methods and procedures used in purification including conversion to specific derivatives or complexes and regeneration of the original material in a much
The book also outlines recent deve nes tmatorial chedstry, solid support chemistry, fluorous chemistry) and the corresponding purification procedures th& will provide many of the commercially supplied chemical substances in years to come. Additionally, interesting perspective about the future of purification is provided by the authors, based on their years of experience. The bulk of the book contains purification procedures (taken from the literature) of individual entries for commercially available organic compounds, inorganic and metal-organic compounds and biochemical and related compounds respectively The entries are accessible in alphabetical order, and in most cases synonymous names and/or abbreviations are included as the CAS (Chemical Abstracts Service) Registry Numbers. The physical properties have been entered, such as the molecular
weight, melting and boiling points, and specific rotations in substances are optically active. Rapid purification procedures for common solvents have also been included after the respective extensive procedures.
New to this edition, the ionisation constants in the form of pK have been entered for ionisable compounds. These are followed by procedures, used to purify the substances, in most cases to analytical purity. An index of CAS Registry Numbers with the respective page numbers of the entries has been added as well, making it easy to locate any substance ikespective of which chapter it is in, and also rapidly telling the reader whether there is a purification procedure for that s u m in this book.
The only complete source that covers the purification of laboratory chemicals that are commertially available in such an easy-to-use format
- Provides purification procedures for commercially available chemicals and biochemicals
- Includes an extremely useful compilation of ionisation constants
Now in its fifth edition, Purification of Laboratory Chemicals continues to ratory scientists with a manual for purifying and increasing the purity of, mode commercially available chemical substances.
The authors have written and revised six chapters that describe the aspects of purification and properties of chemical substances. In addition to detailing physical methods and procedures such as crystallization, distillation, chromatography, etc. , the authors also address cheinical methods and procedures used in purification including conversion to specific derivatives or complexes and regeneration of the original material in a much
The book also outlines recent deve nes tmatorial chedstry, solid support chemistry, fluorous chemistry) and the corresponding purification procedures th& will provide many of the commercially supplied chemical substances in years to come. Additionally, interesting perspective about the future of purification is provided by the authors, based on their years of experience. The bulk of the book contains purification procedures (taken from the literature) of individual entries for commercially available organic compounds, inorganic and metal-organic compounds and biochemical and related compounds respectively The entries are accessible in alphabetical order, and in most cases synonymous names and/or abbreviations are included as the CAS (Chemical Abstracts Service) Registry Numbers. The physical properties have been entered, such as the molecular
weight, melting and boiling points, and specific rotations in substances are optically active. Rapid purification procedures for common solvents have also been included after the respective extensive procedures.
New to this edition, the ionisation constants in the form of pK have been entered for ionisable compounds. These are followed by procedures, used to purify the substances, in most cases to analytical purity. An index of CAS Registry Numbers with the respective page numbers of the entries has been added as well, making it easy to locate any substance ikespective of which chapter it is in, and also rapidly telling the reader whether there is a purification procedure for that s u m in this book.