Louis S. Hegedus (ed. ) An annual publication of satisfactory
methods for the preparation of organic chemicals, volume 79, 2002,
291 p.
Contents
Synthesis of tris(2-perfluorohexylethyl)tin hydride: a highly fluorinated tin hydride with advantageous features of easy purification
1,2-metallate rearrangement: (z)-4-(2-propenyl)-3-octen-1-ol
Dumethyltitanocene
Molybdenum carbonyl-catalyzed alkynol cycloisomerization: preparation of 2-phenyl-2,3-dihidrofuran
Ethyl 3-(p-cyanophenyl)propionate from ethyl 3-iodopropionate and p-cyanophenilzinc bromide
Preparation of n-butyl 4-chlorphenyl sulfide
Synthesis of symmetrical trans-stilbenes by a double heck reaction of (arylazo)amines with vinyltriethoxysilane: trans-4,4'-dibromostilbene
Synthesis and utilization of ini for in situ formation of enetioenriched allenylindium reagents and their addition to aldehydes: (2r,3s,4s)-1-(tert-butyldyphenylsiloxy)-2,4-dimethyl-5-hexyn-3-ol
Asymmetric synthesis of (m)-2-hydroxymethyl-1-(2-hidroxy-4,6-dimethylphenyl)naphtalene via a configurationally unstable biaryl lactone
(R)-3-phenylcyclohexanone
Synthesis of (+)-(1s,2r)- and (-)-(1r,2s)-trans-2-phenylcyclohexanol via shrpless asymmetric dihydroxylation (ad)
Ducyclohexylboron trifluoromethanesulfonate
2-()n-benzyl-n-mesitylenesolfonyl)amino-1-phenyl-1-propyl proprionate
Anti-selective boron-mediated asymmetric aldol reaction of carboxilic esters: synthesis of (2s,3r)-2,4-dimethyl-1,3, -pentanediol
Camphorquinone and camphorquinone monoxime
(2s)-(-)-3-exo(dimethylamino)isoboeol [(2s)-(-)-DAIB]
catalytic enantioselective addition of dialkylzincs to aldehydes using (2s)-(-)-3-exo-(dimethylamino)isoboeol [(2s-DAIB)]
Formation of gamma-keto esters from beta-keto esters: methyl 5,5-dimethyl-4-oxohexanoate
(S)-3-(tert-butyloxycarbonylamino)-4-phenylbutanoic acid
Photo-induced ring expansion of 1-triisopropylsiloxy-1-azidocyclohexane: preparation of epsylon-caprolactam
(3,4,5-trifluorophenyl)boronic acid-catalyzed amide formation from carboxilic acids and amines: n-benzyl-4-phenylbutyramide
Preparation of secondary amines from primary amines via 2-nitrobenzenesulfonamides: n-(4-metoxybenzyl)-3-phenylpropylamine
2-amine-3-fluorobenzoic acid
3-(4-bromobenzoyl)propanoic acid
Nucleophilic aromatic substitution of aryl fluorides by secondary nitriles: preparation of 2-(2-methoxyphenyl)-2-methylpropionitrile
Preparation of 1-(n-benzyloxycarbonyl-(1s)-1-amino-2-oxoethyl)-4-methyl-2,6,7-trioxibicyclo[2.2.2]octane
N-hydroxy-4-(p-chlorophenyl)thiazole-2(3h)-thione
Preparation of 1-butyl-3-methyl imidazolium-based room temperature ionic liquids
4-methoxycarbonyl-2-methyl-1,3-oxazole
[4+3] cycloaddition in water. Synthesis of 2,4-endo, endo-dimethyl-8-oxabicyclo[3.2.1]oct-6-en-one
Contents
Synthesis of tris(2-perfluorohexylethyl)tin hydride: a highly fluorinated tin hydride with advantageous features of easy purification
1,2-metallate rearrangement: (z)-4-(2-propenyl)-3-octen-1-ol
Dumethyltitanocene
Molybdenum carbonyl-catalyzed alkynol cycloisomerization: preparation of 2-phenyl-2,3-dihidrofuran
Ethyl 3-(p-cyanophenyl)propionate from ethyl 3-iodopropionate and p-cyanophenilzinc bromide
Preparation of n-butyl 4-chlorphenyl sulfide
Synthesis of symmetrical trans-stilbenes by a double heck reaction of (arylazo)amines with vinyltriethoxysilane: trans-4,4'-dibromostilbene
Synthesis and utilization of ini for in situ formation of enetioenriched allenylindium reagents and their addition to aldehydes: (2r,3s,4s)-1-(tert-butyldyphenylsiloxy)-2,4-dimethyl-5-hexyn-3-ol
Asymmetric synthesis of (m)-2-hydroxymethyl-1-(2-hidroxy-4,6-dimethylphenyl)naphtalene via a configurationally unstable biaryl lactone
(R)-3-phenylcyclohexanone
Synthesis of (+)-(1s,2r)- and (-)-(1r,2s)-trans-2-phenylcyclohexanol via shrpless asymmetric dihydroxylation (ad)
Ducyclohexylboron trifluoromethanesulfonate
2-()n-benzyl-n-mesitylenesolfonyl)amino-1-phenyl-1-propyl proprionate
Anti-selective boron-mediated asymmetric aldol reaction of carboxilic esters: synthesis of (2s,3r)-2,4-dimethyl-1,3, -pentanediol
Camphorquinone and camphorquinone monoxime
(2s)-(-)-3-exo(dimethylamino)isoboeol [(2s)-(-)-DAIB]
catalytic enantioselective addition of dialkylzincs to aldehydes using (2s)-(-)-3-exo-(dimethylamino)isoboeol [(2s-DAIB)]
Formation of gamma-keto esters from beta-keto esters: methyl 5,5-dimethyl-4-oxohexanoate
(S)-3-(tert-butyloxycarbonylamino)-4-phenylbutanoic acid
Photo-induced ring expansion of 1-triisopropylsiloxy-1-azidocyclohexane: preparation of epsylon-caprolactam
(3,4,5-trifluorophenyl)boronic acid-catalyzed amide formation from carboxilic acids and amines: n-benzyl-4-phenylbutyramide
Preparation of secondary amines from primary amines via 2-nitrobenzenesulfonamides: n-(4-metoxybenzyl)-3-phenylpropylamine
2-amine-3-fluorobenzoic acid
3-(4-bromobenzoyl)propanoic acid
Nucleophilic aromatic substitution of aryl fluorides by secondary nitriles: preparation of 2-(2-methoxyphenyl)-2-methylpropionitrile
Preparation of 1-(n-benzyloxycarbonyl-(1s)-1-amino-2-oxoethyl)-4-methyl-2,6,7-trioxibicyclo[2.2.2]octane
N-hydroxy-4-(p-chlorophenyl)thiazole-2(3h)-thione
Preparation of 1-butyl-3-methyl imidazolium-based room temperature ionic liquids
4-methoxycarbonyl-2-methyl-1,3-oxazole
[4+3] cycloaddition in water. Synthesis of 2,4-endo, endo-dimethyl-8-oxabicyclo[3.2.1]oct-6-en-one