Химия и химическая промышленность
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Mohrig J.R., Hammond C.N., Schatz R.F. Techniques in Organic Chemistry. Miniscale, Standard Microscale, and Williamson Microscale
3rd ed. W.H.Freeman and Company. 2010. 487 p.

Techniques in Organic Chemistry is the most comprehensive presentation of lab techniques available for organic chemistry students—and the least expensive. This book is intended to serve as a laboratory textbook of experimental techniques for all students of organic chemistry. It is written to provide effective support for guided-inquiry and design-based experiments and projects, as well as for traditional lab experiments. Techniques in Organic Chemistry combines specific instructions for 3 different kinds of laboratory glassware (miniscale, standard-taper microscale, Williamson microscale). It offers extensive coverage of spectroscopic techniques and a strong emphasis on safety issues. It can be used in conjunction with any lab experiments to provide the background and skills necessary for mastering the organic chemistry laboratory.

The techniques manual may be purchased separately, or it can be packaged with either version of Mohrig’s Mode Projects and Experiments in Organic Chemistry or with an instructor’s own experiments through Freeman Custom Publishing.

Contents

Introduction to the Organic Laboratory

Safety in the Laboratory
Protecting the Environment
Laboratory Notebooks and Prelaboratory Information

Carrying out Chemical Reactions

Laboratory Glassware
Measurements and Transferring Reagents
Heating and Cooling Methods
Assembling a Reaction Apparatus
Computational Chemistry
Designing a Chemical Reaction

Separation and Purification Techniques

Filtration
Extraction
Drying Organic Liquids and Recovering Reaction Products
Boiling Points and Distillation
Melting Points and Melting Ranges
Recrystallization
Specialized Techniques

Chromatography

Thin-Layer Chromatography
Liquid Chromatography
Gas Chromatography

Spectroscopic Methods

Infrared Spectroscopy
Nuclear Magnetic Resonance Spectroscopy
13C and Two-Dimensional NMR Spectroscopy
Mass Spectrometry
Ultraviolet and Visible Spectroscopy
Integrated Spectroscopy Problems
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